Hull - Refurb 140 Sq.Ft. Freeze Dryer

Fast Delivery: Refurbished 140 Sq.Ft. Freeze Dryer, Model: 140FS275-SS25C, Yr. 1996

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  • 140 Reburbished Hull

    140 Reburbished Hull

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    • Hull Model: 140FS275-SS25C, Yr. 1996 Lyophilizer/Freeze Dryer Refurbished
    • 12 Week Delivery Estimated cGMP
    • Optional SIP, CIP
    • Internal 276 Kg Condenser, Rated @ 24hrs  

    Price: $695,000 USD

      Lyo Specifications

       Chamber:

      Inside: 86 in. Wide x 67 in. Deep x 62 in. High

      Shelves Size: 48 in. Wide x 60 in. Deep Area: 140 Sq. Ft. 

      Clearance between shelves

      Normal shelf clearance: 7 usable shelves with a clearance of 5 ½  in. between shelves.

      Latched shelf position: 3 usable shelves with a clearance of 11 in. between shelves and 1 shelf with a clearance of 5 ½  in. between the shelf.

       

      Stoppering Mechanism:

      Hydraulic I Downward Movement

       

      Materials of Construction:

      Chamber: 316L stainless steel

      Chamber door: 316L stainless steel, water-cooled

      Shelves: 316L stainless steel

        

       

      Condenser: Internal

      8 plates Ice Capacity: 275 liters A. Steam and I or Hot Gas Defrost

       

      Materials of Construction

      Condensing Plates: 304L stainless steel

        

      Mechanical: See upgradesunder "Option Components"

       

      Electrical:

      460 Volts, 3 phase 60 cycle

      Stepdown Transformer for 115 Volt, 1 Phase 60 Cycle Control Circuit \Service

      Amperage Required: 165 amps

       

       

      Utilities:

      Cooling Water-150 GPM minimum to 255 GPM Max. at 75 degrees

      F Sterilization Medium-Clean Steam

      Compressed Air-80 to 110 PSIG max. (approx 0.2 SCFM)

      Condensing Water

      • Compressor Inlet- 120 GPM at 85 degrees F water temp. max.
      • Compressor Outlet- 120 GPM at 95 degrees F water temp. max.

       

      Steam 

      Chamber Sterilization - approx. 490 lb/hr for 1 hour heat- up to 260F

      Condensing Plate Defrost- approx. 330 lb I hr for 1 hour defrost of 275 liters of ice from -70 degrees C to +20 degrees CSystem rates:

      • Shelf Temp Range -50 degrees to +70 degrees
      • C Condenser Temp at Blankoff < -70 degrees C
      • Vacuum Blankoff < 50 microns Leak rate< 5 microns/minute

       

       

      Upgrades (new components unless noted)

       

      Refrigeration/circulation Skid

      1       Refrigeration compressors

      1.1                (2) 30hp two stage semi-hermetic Carlyle main compressors with new:  

      1.1.1                Shell and tube water cooled condenser with regulating valve.

      1.1.2                Plate sub-cooler.

      1.1.3                Oil separator.

      1.1.4                Suction accumulator.

      1.1.5                Oil level/ return sight glass and drain valve.

      1.1.6                Crankcase heater.

      1.1.7                De-super heating circuit.

      1.1.8                Refrigerant level and moisture indicating sight glasses.

      1.1.9                Filter I dryer block assemblies.

       

      1.1.10            Pump down system.

      1.1.11            Mechanical pressure safeties.

      1.1.12            Compressor pressure gauge manifold.  

      1.1.13            Insulate with 3/4" urethane or current standard.  

      1.2                       (1) 20hp two stage semi-hermetic Carlyle shelf compressor with new:

      1.2.1                Shell and tube water cooled condenser with regulating valve.

      1.2.2                Plate sub-cooler.

      1.2.3                Oil separator.

      1.2.4                Suction accumulator.

      1.2.5                Oil level/ return sight glass and drain valve.

      1.2.6                Crankcase heater.

      1.2.7                De-super heating circuit.

      1.2.8                Refrigerant level and moisture indicating sight glasses.

      1.2.9                Filter I dryer block assemblies.

      1.2.10            Pump down system. Mechanical

      1.2.11            pressure safeties. Compressor

      1.2.12            pressure gauge manifold.

       1.1.13            Insulate with 3/4" urethane or current standard.

       

      2       Refrigeration components

      2.1                (3)  Liquid line solenoid valves and (3) low temperature thermostatic expansion valves for shelf cooling circuits.

      2.2                (2)  Liquid line solenoid valves and (2) low temperature thermostatic expansion valves for condenser cooling circuits.

      2.3                Insulated with 3/4" urethane or current standard.  

       

      3                  Circulation system

      3.1                (1) Centrifugal circulation pump:

      3.1.1              Inlet/Outlet pressure gauges.

      3.1.2              Isolation valve.

      3.2                (3) Plate type circulation fluid heat exchangers sized for new compressors.

      3.3                (1) Four core filter/dryer assembly with

      3.3.1             Inlet/outlet pressure gauges

      3.3.2             Isolation valves

      3.4                Circulation charging/draining system.

      3.5                30kw circulation heater.

      3.6                Insulated with 3/4" urethane or current standard.

       

       4      Frame and skid

      4.1     Single frame constructed of carbon steel and epoxy coated.

       

      5       Electrical

      5.1                All intra-skid wiring with:

      5.1.1             Component connections in water tight conduit and cable.

      5.1.2             Signal wiring in PVC jacketed shielded cable.

        

       6       Miscellaneous

      6.1                System will be fully pressure tested.

      6.2                Compressors to be filled with POE oil.

      6.3                Systems to be charged with R-507, or 404A refrigerant.

      6.4                Circulation system to be charged with Silicone Oil.

       

      Vacuum Pump System

      1      Pumps

      1.1               (2) Leybold 0658  vacuum pumps (oil mist separators are included).

      1.2               (1) Leybold WSU blower

      1.3               New 3" air actuated isolation valves.  

      1.4               New 3" vibration eliminators.  

       

      2      Frame and skid

      2.1               Single frame constructed of carbon steel and epoxy coated.  

       

      3      Vessel connection

      3.1               Carbon steel pipe epoxy coated.

      3.2               New 6" air actuated condenser vacuum valve.

      3.3               Oil drip line.  Vessel  

       

      4     Chamber/Condenser

      4.1         New %" air actuated vacuum break valve.

      4.2         New MKS proportional valve with a solenoid isolation valve for vacuum control.

      4.3         New 2" air actuated drain valve.

      4.4         Level and evenly space shelves.

      4.5         Full re-insulation of vessel with outer PVC jacket.

       

      Control System

      Mechanical control cabinet

       1.1    New NEMA 12 enclosure (to be mounted on the refrigeration skid) to house the following devices:

      • 1.1.1      MCC disconnect.
      • 1.1.2      MCC venting and lighting.
      • 1.1.3      Wire distribution and protection devices.  
      • 1.1.4      Allen-Bradley PLC.
      • 1.1.5      Motor controls and motor protectors.  
      • 1.1.6      Heater controller and safety.
      • 1.1.7      Wire terminals.
      • 1.1.8      Power supplies.
      • 1.1.9      Ethernet switch.
      • 1.1.10  8" Operator Control Terminal.

       

      2       HMI (Human Machine Interface)

      2.1     Installation of the Lyo-Control HMI.

       

      3       New Allen-Bradley Compactlogix programmable logic controller system.

                3.11769-L33ER  CPU.

                3.21769 series 1/0.

      4       Installation of (4) Acto De precision power supplies.

      5       Installation of a new Control Concepts SCRs for heater control.

      6       Installation of a new MKS 628 capacitance manometers for chamber low pressure measurement.

      7       Installation of a new MKS 1249A signal retransmitter.  The 1249A retransmits the vacuum control signal of the PLC from 4-20ma to 0-120ma for the new MKS 248 proportional control valves.

      8       Installation of a new Omega 615 pressure transducer for chamber pressure (PSIA) measurement.

      9       Installation of a remote 1/0 system.

               9.1     New NEMA 12 enclosure (to be mounted on the chamber vessel) to house the following devices:

      • 9.1.1      Opto-22 remote 1/0.
      • 9.1.2      Venting and lighting.
      • 9.1.3      Wire distribution and protection devices.
      • 9.1.4      Power supply.
      • 9.1.5      Wire terminals.

      10   Programming and setup for above controllers.  Programs to include:

      • 10.1     Standard Freeze Dry cycle.
      • 10.2     Condenser Defrost cycle.
      • 10.3     System Plant Test cycle, including Leak Test.
      • 10.4     Message and alarm generation.
         Motor alarms
         Analog Input failure alarms
          -  Vacuum alarms
          -  Condenser temperature alarms
          - Shelf temperature alarms
      • 10.5     Bumpless transfer of devices from Auto to Manual.
      • 10.6      HMI programming and screen development.

       

      Installation

      1.  Installation isnot included.

       

      Testing

      1        Factory acceptance testing to include the following:

      1.1.      Shelf freeze rates and dwells.

      1.2.      Condenser freeze rates.

      1.3.      Evacuation rates and dwells.

      1.4.      Sublimation rates and condenser capacity.

      1.5.      Automated cycles.

      1.6.      Alarm conditions.

      1.7.      HMI screen verification.

       

      Documentation

      1      Documentation to include the following:

      1.1     As built P&ID schematics.

      1.2     As built electrical schematics.

      1.3     As built general arrangement.

      1.4     Operation manuals.

      1.5     Spare parts lists.

      1.6     PLC program.

      1.7     HMI program.

      1.8     Calibration Certificates.  

      1.9     All OEM documentation.

       

      Options

      1      Options for this Lyo are the following:

      1.1     SIP (without jacket cooling).

      1.2     CIP upgrade.

      1.3     Screw compressor upgrade.

      1.4     Automatic stoppering.  

      1.5     24vac/vdc controls.

      1.6     Remote 1/0 upgrade to Allen-Bradley Point 1/0. 

        

      Warranty

      1.     Main new components - Manufacturer's warranty

      2.     Fabrication- 1 year from shipment.